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A synthetic procedure has been developed for the preparation of a new type of macrocycle in which the ferrocene unit is appended to an O-N-P-macrocycle or it is incorporated within the macrocyclic unit. The methodology is based on the Staudinger reaction of a bis-azide with the appropriate diphosphine.

Preparation of heteromacrocycles bearing two tetra-coordinate phosphorus atoms and at least two ferrocene units