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Two series of functionalized imidazothiazolotriazine derivatives were synthesized via the condensation of imidazo[4,5- e ]-1,2,4-triazine-3-thiones with acetylenedicarboxylic acid dimethyl and diethyl esters (DMAD and DEAD) and subsequent base-catalyzed rearrangement of the obtained imidazo[4,5- e ]thiazolo[3,2- b ]-1,2,4-triazines into regioisomeric imidazo[4,5- e ]thiazolo[2,3- c ]-1,2,4-triazine derivatives.

beilstein journal of organic chemistry

Synthesis of functionalized imidazo[4,5-e]thiazolo[3,2-b]triazines by condensation of imidazo[4,5-e]triazinethiones with DMAD or DEAD and rearrangement to imidazo[4,5-e]thiazolo[2,3-c]triazines