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The reported flow-batch approach enables the easy preparation of 2 H -azirines and their stereoselective transformation into highly functionalized NH -aziridines, starting from vinyl azides and organolithium compounds. The protocol has been developed using cyclopentyl methyl ether (CPME) as an environmentally benign solvent, resulting into a sustainable, safe and potentially automatable method for the synthesis of interesting strained compounds.

beilstein journal of organic chemistry

A sustainable strategy for the straightforward preparation of 2<i>H</i>-azirines and highly functionalized <i>NH</i>-aziridines from vinyl azides using a single solvent flow-batch approach

A sustainable strategy for the straightforward preparation of 2H-azirines and highly functionalized NH-aziridines from vinyl azides using a single solvent flow-batch approach