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A cascade oxidative trifluoromethylthiolation and cyclization of N -[(3-aryl)propioloyl]indoles with AgSCF 3 is described. This protocol allows for the synthesis of novel bis(trifluoromethylthiolated) or trifluoromethylthiolated pyrrolo[1,2- a ]indol-3-ones in moderate to good yields. Mechanistic investigations indicated that radical processes were probably involved in these transformations.

Cascade trifluoromethylthiolation and cyclization of N-[(3-aryl)propioloyl]indoles