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The efficient hydrohydrazidation of terminal ( 6a - r , 18 examples, 0.1-0.2 mol % [(NHC)Au(NTf 2 )], T = 60 °C) and internal alkynes ( 7a - j , 10 examples, 0.2-0.5 mol % [(NHC)Au(NTf 2 )], T = 60-80 °C) utilizing a complex with a sterically demanding bispentiptycenyl-substituted NHC ligand and the benign reaction solvent anisole, is reported.

Efficient [(NHC)Au(NTf2)]-catalyzed hydrohydrazidation of terminal and internal alkynes

Efficient [(NHC)Au(NTf₂)]-catalyzed hydrohydrazidation of terminal and internal alkynes