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An intermolecular radical addition, using photoredox catalysis, to allenamides and allencarbamates is reported. This transformation synthesizes N -acyl- N' -aryl- N , N' -allylaminals, and proceeds by a conjugated N -acyliminium intermediate that previously has principally been generated by electrophilic activation methods. The radical adds to the central carbon of the allene giving a conjugated N -acyliminium that undergoes nucleophilic addition by arylamines and alcohols.

beilstein journal of organic chemistry

A complementary approach to conjugated <i>N</i>-acyliminium formation through photoredox-catalyzed intermolecular radical addition to allenamides and allencarbamates

A complementary approach to conjugated N-acyliminium formation through photoredox-catalyzed intermolecular radical addition to allenamides and allencarbamates