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Dirhodium(II) complex-catalyzed [3 + 2] reactions between N -arylaminocyclopropanes and alkyne derivatives are described. The cycloaddition products proved to be versatile synthetic intermediates. trans -Cyclic β-amino acids and derivatives thereof can be conveniently synthesized using this cycloaddition protocol.

Dirhodium(II)-catalyzed [3 + 2] cycloaddition of N-arylaminocyclopropane with alkyne derivatives