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In this study, M βα  X-ray production cross-sections and average M-shell fluorescence yields were determined by using EDXRF at 5.96 keV for Pt, Au and Tl compounds. The photo-peak areas were used for the measurement of M X-ray production cross-sections and also other parameters. The obtained values were compared with the theoretical values in the literature to explain the changes in parameters. It was obtained that the changes were resulted from the electronegativity differences between Pt, Br and O in Pt compounds and Au, Br and O in Au compounds. As for Tl compounds, it was obtained different results and attributed to both of the charge transfer from one element to another and polarizability mechanisms of Tl.

M shell Fluorescence Parameters of Pt, Au and Tl Compounds with Oxygen and Bromide