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In this work, a fuzzy logic model was developed to elucidate the extraction performance of high-pressure CO2 + H2O compared with traditional H2O extraction and aqueous ethanol extraction. The high-pressure CO2 + H2O group acquired the highest comprehensive score considering yield, quality and stability. Both targeted and untargeted metabolomics results proved that the polarity of water was slightly modified; in particular, with the evidence from the untargeted metabolomics data, a higher proportion of water-insoluble compounds (2-methylindole, 3-formylindole, guanine, tyrosine and tryptophan) obtained by high-pressure CO2 + H2O extraction compared with traditional H2O extraction has been reported for the first time. Finally, the “3I” extraction mechanism of high-pressure CO2 + H2O is proposed, which offers an improvement in the solid–liquid mass transfer efficiency of phytochemicals, improving the polarity of solution and the isolation of O2.

Evaluation Study on Extraction of Anthocyanins from Red Cabbage Using High Pressure CO2 + H2O: A Fuzzy Logic Model and Metabolomic Analysis