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Anionic polymerization techniques were employed for the synthesis of linear polystyrene (PS) and block copolymer of PS and polyisoprene (PI) PS- b -PI bearing end hydroxyl groups. Following suitable organic chemistry transformation, the -OH end groups were converted to moieties able to form complementary hydrogen bonds including 2,6-diaminopurine, Dap, thymine, Thy, and the so-called Hamilton receptor, Ham. The formation of hydrogen bonds was examined between the polymers PS-Dap and PS- b -PI-Thy, along with the polymers PS-Ham and PS- b -PI-Thy. The conditions under which supramolecular triblock copolymers are formed and the possibility to form aggregates were examined both in solution and in the solid state using a variety of techniques such as 1 H-NMR spectroscopy, size exclusion chromatography (SEC), dilute solution viscometry, dynamic light scattering (DLS), thermogravimetric analysis (TGA), differential thermogravimetry (DTG), and differential scanning calorimetry (DSC).

polymers

Supramolecular Triblock Copolymers Through the Formation of Hydrogen Bonds: Synthesis, Characterization, Association Effects in Solvents of Different Polarity