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Electrochemical polymerisation is reported to be a method for readily producing copolymers of various conjugated molecules. We employed this method for mixtures of indole, carbazole or fluorene with 3-hexylthiophene (HT), in order to obtain their soluble copolymers. Although polymer films were obtained, infrared (IR) and Raman investigations showed that instead of the expected linear copolymers, polyindole and polycarbazole N -substituted with HT, as well as a poly(3-hexylthiophene) (PHT)/polyfluorene blend were produced instead. Boron trifluoride diethyl etherate was also used in an attempt to promote copolymerisation, but the produced deposits were found to be highly degraded.

The Different Outcomes of Electrochemical Copolymerisation: 3-Hexylthiophene with Indole, Carbazole or Fluorene