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TiO₂ hollow spheres modified with spatially separated Ag species and RuO₂ cocatalysts have been prepared via an alkoxide hydrolysis-precipitation method and a facile impregnation method. High-resolution transmission electron microscopy studies indicate that Ag species and RuO₂ co-located on the inner and outer surface of TiO₂ hollow spheres, respectively. The resultant catalysts show significantly enhanced activity in photocatalytic hydrogen production under simulated sunlight attributed to spatially separated Ag species and RuO₂ cocatalysts on TiO₂ hollow spheres, which results in the efficient separation and transportation of photogenerated charge carriers.

Design and Synthesis of TiO2 Hollow Spheres with Spatially Separated Dual Cocatalysts for Efficient Photocatalytic Hydrogen Production