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Cu 3 (BTC) 2 (BTC: 1,3,5-benzenetricarboxylate) as a heterogeneous catalyst in the presence of cesium carbonate as a base is reported for the borylation of α,β-conjugated enones by bis(pinacolato)diboron (B 2 pin 2 ). According to the hot-filtration test, Cu 3 (BTC) 2 is acting as a heterogeneous catalyst. Further, Cu 3 (BTC) 2 exhibits a wide substrate scope and can be reused in consecutive runs, maintaining a crystal structure as evidenced by powder X-ray diffraction (XRD). A suitable mechanism is also proposed for this transformation using Cu 3 (BTC) 2 as catalyst.

α,β-Enone Borylation by Bis(Pinacolato)Diboron Catalyzed by Cu3(BTC)2 Using Cesium Carbonate as a Base