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A binary carbonate salt eutectic (Li 2 CO 3 -K 2 CO 3 )-based nanofluid was in situ synthesized by mixing with a precursor material, aluminum nitrate nonahydrate (Al(NO 3 ) 3 ·9H 2 O). Thermal decomposition of the precursor was successfully carried out to synthesize alumina (Al 2 O 3 ) nanoparticles at 1 wt.% concentration. A thermogravimetric analysis (TGA) confirmed a complete thermal decomposition of aluminum nitrate nonahydrate to alumina nanoparticles. A transmission electron microscope (TEM) was employed to confirm the size and shape of the in situ formed nanoparticles; the result showed that they are spherical in shape and the average size was 28.7 nm with a standard deviation of 11.7 nm. Electron dispersive X-ray spectroscopy (EDS) confirmed the observed nanoparticles are alumina nanoparticles. A scanning electron microscope (SEM) was employed to study microstructural changes in the salt. A differential scanning calorimeter (DSC) was employed to study the heat capacity of the in situ synthesized nanofluid. The result showed that the heat capacity was enhanced by 21% at 550 °C in comparison with pure carbonate salt eutectic. About 10-11 °C decrease of the onset melting point of the binary carbonate salt eutectic was observed for the in situ synthesized nanofluids.

In Situ Synthesis of Alumina Nanoparticles in a Binary Carbonate Salt Eutectic for Enhancing Heat Capacity