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Photocatalytic utilization of CO 2 in the production of value-added chemicals has presented a recent green alternative for CO 2 fixation. In this regard, three FeNbO 4 /NH 2 -MIL-125(Ti) composites of different mole ratios were synthesized, characterized using Powder X-ray diffraction (PXRD), UV-vis diffuse reflectance spectroscopy (UV-Vis DRS), Brunauer-Emmett-Teller (BET), Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray (EDX). PXRD patterns confirm the co-existence of the parent components in the prepared composites. Moreover, the surface area increased as the mole percent of NH 2 -MIL-125(Ti) in the composites increased due to the large surface area of NH 2 -MIL-125(Ti). Prepared composites were investigated for the photocatalytic insertion of CO 2 into propylene oxide. FeNbO 4(75%) /NH 2 -MIL-125(Ti) (25%) showed the highest percent yield of 52% compared to the other two composites. Results demonstrate the cooperative mechanism between FeNbO 4 and NH 2 -MIL-125(Ti) and that the reaction proceeded photocatalytically.

Photocatalytic Activities of FeNbO4/NH2-MIL-125(Ti) Composites toward the Cycloaddition of CO2 to Propylene Oxide