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Eight mixed-ligand coordination networks, [Cd(2-aba)(NO 3 )(4-bphz) 3/2 ] n ·n(dmf) ( 1 ), [Cd(2-aba) 2 (4-bphz)] n ·0.75n(dmf) ( 2 ), [Cd(seb)(4-bphz)] n ·n(H 2 O) ( 3 ), [Cd(seb)(4-bpmhz)] n ·n(H 2 O) ( 4 ), [Cd(hpa)(3-bphz)] n ( 5 ), [Zn(1,3-bdc)(3-bpmhz)] n ·n(MeOH) ( 6 ), [Cd(1,3-bdc)(3-bpmhz)] n ·0.5n(H 2 O)·0.5n(EtOH) ( 7 ), and [Cd(NO 3 ) 2 (3-bphz)(bpe)] n ·n(3-bphz) ( 8 ) were obtained by interplay of cadmium nitrate tetrahydrate or zinc nitrate hexahydrate with 2-aminobenzenecarboxylic acid (H(2-aba)), three dicarboxylic acids, sebacic (decanedioic acid, H 2 seb), homophthalic (2-(carboxymethyl)benzoic acid, H 2 hpa), isophthalic (1,3-benzenedicarboxylic acid, H 2 (1,3-bdc)) acids, bis(4-pyridyl)ethane (bpe) and with four azine ligands, 1,2-bis(pyridin-4-ylmethylene)hydrazine (4-bphz), 1,2-bis(1-(pyridin-4-yl)ethylidene) hydrazine (4-bpmhz), 1,2-bis(pyridin-3-ylmethylene)hydrazine (3-bphz), and 1,2-bis(1-(pyridin-3-yl) ethylidene)hydrazine (3-bpmhz). Compounds 1 and 2 are 1D coordination polymers, while compounds 3 - 8 are 2D coordination polymers. All compounds were characterized by spectroscopic and X-ray diffraction methods of analysis. The solvent uptakes and stabilities to the guest evacuation were studied and compared for 1D and 2D coordination networks. The de-solvated forms revealed a significant increase of emission in comparison with the as-synthesized crystals.

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From 1D to 2D Cd(II) and Zn(II) Coordination Networks by Replacing Monocarboxylate with Dicarboxylates in Partnership with Azine Ligands: Synthesis, Crystal Structures, Inclusion, and Emission Properties