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Large-size, superparamagnetic, and highly magnetic Fe 3 O 4 @PDA core-shell submicrosphere-supported nano-palladium catalysts were prepared in this study. Dopamine was encapsulated on the surface of Fe 3 O 4 particles via self-polymerization and then protonated to positively charge the microspheres. PdCl 4  2- was dispersed on the surface of the microspheres by positive and negative charge attraction and then reduced to nano-palladium. With air as oxidant, the catalyst can successfully catalyze the dehydrogenation of benzyl alcohols to produce the corresponding aldehydes at 120 °C.

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Preparation of Large-Size, Superparamagnetic, and Highly Magnetic Fe3O4@PDA Core–Shell Submicrosphere-Supported Nano-Palladium Catalyst and Its Application to Aldehyde Preparation through Oxidative Dehydrogenation of Benzyl Alcohols