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The precipitation behavior of the orthorhombic (O) phase during the slow cooling aging treatment of Ti-22Al-25Nb (at.%) alloy was investigated by microstructural characterization. Then the effect of O phase precipitation on the tensile properties was studied by room-temperature tensile tests. The results showed that the precipitation of the O phase transformed from both grain boundaries and intragranular to only grain boundaries with the temperature increasing. The nucleation mechanism of the O phase from intergranular is composed of sympathetic nucleation and interface instability nucleation. In addition, the results of tensile tests indicated that the ultimate tensile strength of the alloy decreases as the precipitation of the O phase increases. Meanwhile, from the tensile results, it is concluded that the optimum heat treatment process is slow cooling after aging at 950 °C for 1 h.

Precipitation Behavior of Orthorhombic Phase in Ti-22Al-25Nb Alloy during Slow Cooling Aging Treatment and Its Effect on Tensile Properties