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This article describes the successful application of the DOSY method for the separation and analysis of the α- and β-anomers of carbohydrates with different diffusion coefficients. In addition, the DOSY method was found to effectively separate two kinds of glucopyranosides with similar aglycon structures from a mixture

Separation of the α- and β-Anomers of Carbohydrates by Diffusion-Ordered NMR Spectroscopy