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Inorganic-organic hybrid crystals containing α-octamolybdate (Mo 8 ) or hexamolybdate (Mo 6 ) were isolated by using hexadecyltrimethylammonium (C 16 ) surfactant. The packing mode of the inorganic layers depended on a difference in the polyoxomolybdate molecular structure. The structure for both crystals consisted of alternate stacking of C 16  organic bilayers and polyoxomolybdate inorganic layers with a periodicity of 24.4–24.6 Å. However, the C 16 -Mo 8  crystals contained Mo 8  monolayers, while the C 16 -Mo 6  crystals contained Mo 6  bilayers. These lattice structures for the polyoxometalate/organic hybrid will be designed by the molecular structures of polyoxometalate.

Controllable Layered Structures in Polyoxomolybdate-Surfactant Hybrid Crystals