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The laser power bed fusion approach has been successfully employed to manufacture Mo(Si,Al) 2 -based composites through the selective laser melting of a MoSi 2 -30 wt.% AlSi10Mg mixture for high-temperature structural applications. Composites were manufactured by leveraging the in situ reaction of the components during printing at 150-300 W laser power, 500-1000 mm·s -1 laser scanning speed, and 100-134 J·mm -3 volumetric energy density. Microcomputed tomography scans indicated a negligible induced porosity throughout the specimens. The fully dense Mo(Si 1-x ,Al x ) 2 -based composites, with hardness exceeding 545 HV1 and low roughness for both the top (horizontal) and side (vertical) surfaces, demonstrated that laser-based additive manufacturing can be exploited to create unique structures containing hexagonal Mo(Si 0.67 Al 0.33 ) 2 .

In Situ Mo(Si,Al)2-Based Composite through Selective Laser Melting of a MoSi2-30 wt.% AlSi10Mg Mixture