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KTaO 3 /Au hetero-nanostructures were synthesized by in-situ reduction of HAuCl 4 on the surface of hydrothermally-grown KTaO 3 sub-micron cubes. The concentration of Au source was found to be a critical factor in controlling the hetero-nucleation of Au nanoparticles on the surface of KTaO 3 sub-micron cubes. Loading of Au particles on KTaO 3 nanocrystals enriched KTaO 3 additional UV-vis absorption in the visible light region. Both KTaO 3 and KTaO 3 /Au nanocrystals were shown to be active in the photo-degradation of p-nitrophenol, while the loading of Au on KTaO 3 clearly improved the photo-degradation efficiency of p-nitrophenol compared to that on bare KTaO 3 nanocrystals, probably due to the improved light absorption and charge separation.

In-Situ Growth of Au on KTaO3 Sub-Micron Cubes via Wet Chemical Approach for Enhanced Photodegradation of p-Nitrophenol