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The title compound 1 was synthesized by the coupling reaction of 2,3,4,6-tetra-O-benzyl-1-C-phenyl-α-D-glucopyranose (2) with 2,3,4,6-tetra-O-benzyl-D-glucopyranose (3) in the presence of 5 mol% bismuth(III) triflate in dichloromethane at 0 °C

2,3,4,6-Tetra-O-benzyl-1-C-phenyl-α-D-glucopyranosyl 2,3,4,6-Tetra-O-benzyl-α-D-glucopyranoside