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The title compound 1 was synthesized by the coupling reaction of 6,7,8,10-tetra-O-benzyl-1,2,3,4-tetradeoxy-α-D-gluco-dec-5-ulopyranose (2) with 2,3,4,6-tetra-O-benzyl-D-glucopyranose (3) in the presence of 5 mol% bismuth(III) triflate in dichloromethane at 0 °C

6,7,8,10-Tetra-O-benzyl-1,2,3,4-tetradeoxy-α-D-gluco-dec-5-ulopyranosyl 2,3,4,6-Tetra-O-benzyl-α-D-glucopyranoside