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Reaction of 5-chloro-1,3-dimethyl-1H-pyrazole with I2/HIO3 in refluxing acetic acid gives the title compound in good yield. Detailed spectroscopic data (1H NMR, 13C NMR, 15N NMR, IR, MS) are presented

5-Chloro-4-iodo-1,3-dimethyl-1H-pyrazole