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4-(4-(dimethylamino)phenyl)-5-acetyl-6-phenyl-3,4-dihydropyrimidin-2(1H)-thione was prepared from benzoxyacetone (1) (1.62 g, 10 mmol), N,N-dimethylaniline (2) (1.21 g, 10 mmol) and thiourea (3) (1.140 g, 15 mmol) in dichloromethane (15 mL) as solvent using KF/Al2O3 (5 g) as a catalysis.[...]

Synthesis of 4-(4-(dimethylamino)phenyl)-5-acetyl-6-phenyl-3,4-dihydropyrimidin-2(1H)-thione