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A solution of furfurylamine[1] (9.77 g, 100 mmol) in tert-butylmethyl ether[2] (MTBE, 50 mL) was made in a 250-mL four-necked flask, fitted with two dropping funnels and an immersion thermometer, and cooled in an ice/salt bath to -15 °C.[...]

N-Furan-2-ylmethyl-4-methyl-benzenesulfonamide (N-Furfuryl-p-toluenesulfonamide)