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Ethyl 4‐(butylamino)‐3‐nitrobenzoate upon “one‐pot” nitro‐reductive  cyclization using sodium dithionite and substituted aldehyde in dimethyl sulphoxide affords ethyl 1‐butyl‐2‐(2‐hy‐ droxy‐4‐methoxyphenyl)‐1H‐benzo[d]imidazole‐5‐carboxylate in an 87% yield. The structural char‐ acterization was determined by Fourier‐transfer infrared spectroscopy (FT‐IR), Proton nuclear mag‐ netic resonance (1H‐NMR) , Carbon‐13 nuclear magnetic resonance (13C‐NMR), mass spectrometry, Ultraviolet‐visible(UV‐Vis), photoluminescence  (PL),  thin‐film solid emission spectra, cyclic volt‐ ammetry (CV) and thermogravimetric (TGA) analysis. Molecular electrostatic potential (MEP) was studied to determine the reactive sites of the molecule.

Ethyl 1-Butyl-2-(2-hydroxy-4-methoxyphenyl)-1H-benzo[d]imidazole-5-carboxylate