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The synthesis of photoswitchable azo -dibenzo[ b , f ]oxepine derivatives and microtubule inhibitors were described. Subsequently, we examined the reaction of methoxy derivative 3-nitrodibenzo[ b , f ]oxepine with different aldehydes and in the presence of BF 3 ·OEt 2 as a catalyst. Our study provided a very concise method for the construction of the azo -dibenzo[ b , f ]oxepine skeleton. The analysis of products was run using experimental and theoretical methods. Next, we evaluated the E / Z isomerization of azo -dibenzo[ b , f ]oxepine derivatives, which could be photochemically controlled using visible-wavelength light.

Synthesis and Investigations of Building Blocks with Dibenzo[b,f] Oxepine for Use in Photopharmacology