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Novel cyclohexapeptide has been synthesized by replacing the unusual amino acids (dolaphenvaline and dolaphenleuine) of dolastatin 16 with (±)-cis-exo-norbarnane and phenyl alanine amino acids. Novel cyclic hexapeptide alongwith dimers, tetramers composed of alternating L-proline subunits have been synthesized in solution phase and well characterized.

&lt;strong&gt;Synthesis of novel &lt;/strong&gt;(&amp;plusmn;)-&lt;strong&gt;&lt;em&gt;cis-exo&lt;/em&gt;&lt;/strong&gt;&lt;strong&gt;-norbornane amino acid containing cyclic hexapeptide: Analogue of Dolastatin 16 &lt;/strong&gt;