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Iron-doped nickel oxide (Fe0.05Ni0.99) nanoparticles were prepared by ball milling the stoichiometric powder mixture of NiCl2.4H2O and FeCl3.6H2O and citric acid , and calcined at 550 0C for 5 h. The phase composition and the structure of the calcined products were investigated by X-ray diffraction and scanning electron microscopy techniques, respectively. Then the potential of the obtained photocatalyst in degradation of methylene blue dye was studied under visible irradiation.

Synthesis of Fe-doped Nickel oxide nanostructures via a simple mechanochemical route and its application for photocatalytic removing of MB