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SrLi2{Li[CoN2]}, an isostructural variant of Li4SrN2, has been synthesised as black single crystals from a reaction between Li2[(Li,Co)N] and Sr2N, at 973 K using a Li flux in a sealed tantalum ampoule. Single crystal diffraction refinements gave a tetragonal unit cell, which upon closer inspection showed a monoclinic supercell. This supercell allowed, for the first time, the refinement of the occupation of metal atoms along the infinite chains in the structure, resulting in the chemical formula SrLi2{Li0.65Co0.35[Co0.65Li0.35N2]}. This revealed a clear preference for the Li and Co atoms to alternate along the chains. Magnetic measurements showed the sample to be a Curie paramagnet, with Co(I) being in a high-spin S = 1 configuration.

Li and Co Ordering in the Nitridocobaltate(I) SrLi2{Li[CoN2]}