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New radical cation salts (BEDT-TTF)[8,8&#039;,(7)-Cl2(Cl0.09)-3,3&#039;-Co(1,2-C2B9H9.91)(1&#039;,2&#039;-C2B9H10)] (1), (BEDT-TTF)[8,8&#039;-Br0.75Cl1.25-3,3&#039;-Co(1,2-C2B9H10)2] (2), and (BMDT-TTF)4[8,8&#039;-Br1.16(OH)0.72-3,3&#039;-Co(1,2-C2B9H10.06)2] (3) were synthesized, and their crystal structures and electrical conductivities were determined. All the radical cation salts are semiconductors. Compounds 1 and 2 were found to be isostructural, however their electrical conductivities strongly differ (s293 = 2 Ω−1cm−1 and 10−5 Ω−1cm−1, respectively)

New Fulvalenium Salts of Cobalt Bis(dicarbollide): Crystal Structures and Electrical Conductivities