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A novel rare hexa nuclear cadmium(II)–azide cluster, [Cd6(TPA)4(μ3-1,1,3-N3)4(μ2-1,1-N3)6](ClO4)2·2H2O (1) was isolated and structurally characterized, in which the azide ligands reveal μ-1,1,3- and μ-1,1-N3 bridging modes.

Hexnuclear Cadmium(II) Cluster Constructed from Tris(2-methylpyridyl)amine (TPA) and Azides