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We present a preparation method for hollow silica nanocubes with tuneable size and shape in the range required for light scattering studies. Cuprous oxide nanocubes are prepared by a water-assisted polyol method. By adjusting the water content, the size of the nanocubes can be tuned in the range of 40–120 nm. These cubes function as a shape template in the subsequent coating with Stöber silica, resulting in core-shell nanocubes. Dissolving the core with nitric acid results in hollow silica nanocubes with sizes ranging from 80–120 nm and cubicity shape parameters between 3 and 6.5.

Synthesis of Hollow Silica Nanocubes with Tuneable Size and Shape, Suitable for Light Scattering Studies