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A microflow process was developed for Suzuki-Miyaura Couplings (SMCs) in high-pressure and high-temperature (HPHT) water with a small amount of ethanol. Using this approach, an efficient SMC between 4-methylphenylboronic acid and iodobenzene as a model reaction was demonstrated in water medium, in the presence of ppm order PdCl2/NaOH as a simple catalyst/base without any additional ligands, affording the desired products in good yields within <25 s of residence time. The strategy developed for SMCs also demonstrated an aspect of separation by quantitative tracing of 0.1 ppm contaminated Pd with the product, which might be attributed to the low catalyst amount along with the reaction conditions, as well as the immediate membrane separation applied in the sequence.

Rapid Suzuki-Miyaura Couplings with ppm Level of Palladium Catalyst in a High-Pressure and High-Temperature Water System