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1H and 13C{1H} NMR spectra were recorded on JEOL ECX-500 and ECS-400 spectrometers at room temperature. Gas chromatography (GC) analyses were performed on a GL-Sciences GC353B gas chromatograph with a capillary column (GL-Sciences and InertCap Pure WAX). Elemental analyses were carried out at the Microanalysis Center of Kyoto University. Silica-gel column chromatography was carried out by using Wako-gel C-200. The compounds, [Cp*IrCl2]2 (Cp* = -pentamethylcyclopentadienyl) [1] and [Cp*Ir(OH2)3](OTf)2 [2]were prepared according to the literature method. The diol 7c was prepared by the reduction of 2-benzoylbenzoic acid using LiAlH4 [3]. The diols 7e, 7f and 7g were prepared by the reduction of the corresponding dicarboxylic acids using BH3-THF [3]. All other reagents are commercially available and were used as received.

catalysts

Dehydrogenative Transformation of Alcoholic Substrates in Aqueous Media Catalyzed by an Iridium Complex Having a Functional Ligand with α-Hydroxypyridine and 4,5-Dihydro-1H-imidazol-2-yl Moieties