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A novel fluorous hydrazine‐1,2‐bis(carbothioate) was prepared. It showed good catalytic  activity in the synthesis of ‐chloroethers with N‐chlorosuccinimide under mild reaction conditions.  This  fluorous  organocatalyst  could  be  recovered  and  recycled  several  times  with   good purity

A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide