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The general utilization of processing equipment in industry has increased the risk of foreign material contamination. For example, peanut and walnut contaminants in whole wheat flour, which typically a healthy food, are a threat to people who are allergic to nuts. The feasibility of utilizing near-infrared hyperspectral imaging to inspect peanut and walnut powder in whole wheat flour was evaluated herein. Hyperspectral images at wavelengths 950–1700 nm were acquired. A standard normal variate combined with the Savitzky–Golay first derivative spectral transformation was adopted for the development of a partial least squares regression (PLSR) model to predict contamination concentrations. A successive projection algorithm (SPA) and uninformative variable elimination (UVE) for feature wavelength selection were compared. Two individual prediction models for peanut or walnut-contaminated flour, and a general multispectral model for both peanut-contaminated flour and walnut-contaminated flour, were developed. The optimal general multispectral model had promising results, with a determination coefficient of prediction (Rp) of 0.987, and a root mean square error of prediction (RMSEP) of 0.373%. Visualization maps based on multispectral PLSR models reflected the contamination concentration variations in a spatial manner. The results demonstrated that near-infrared hyperspectral imaging has the potential to inspect peanut and walnut powders in flour for rapid quality control.

Evaluation of Near-Infrared Hyperspectral Imaging for Detection of Peanut and Walnut Powders in Whole Wheat Flour