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Two new thio-compounds named aspergerthinol A and B ( 1  and  2 ) and two new monoterpenes named aspergerthinacids A and B ( 3  and  4 ) were isolated from the fungus  Aspergillus  sp. CYH26 from the rhizosphere soil of  Cynanchum bungei  Decne. The structures of compounds were elucidated by spectroscopic data and quantum NMR and ECD calculations. Compounds  1  and  2  represented a new family of sulfur containing natural products with a 3-methyl-4 H -cyclopenta[b]thiophen-4-one skeleton. Compounds  1–4  showed inhibitory activities against nitric oxide (NO) with IC 50  values of 38.0, 19.8, 46.3, and 56.6 μM, respectively.

New Thio-Compounds and Monoterpenes With Anti-inflammatory Activities From the Fungus Aspergillus sp. CYH26