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A new photocatalyst denoted as mTHPC/pCN was prepared by modifying protonated graphitic carbon nitride (pCN) by  meso -tetrahydroxyphenylchlorin (mTHPC). Relevant samples were characterized via various methods including zeta potential measurements, X-ray diffraction, Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy, N 2  adsorption–desorption, transmission electron microscopy, ultraviolet-visible–near-infrared spectroscopy, electrochemical impedance spectroscopy, photocurrent response measurements, electron spin resonance spectroscopy, and phosphorescence spectroscopy. Compared with pCN, mTHPC/pCN shows enhanced absorption in the visible and near-infrared regions and thus higher photocatalytic activity in hydrogen evolution. A possible mechanism for mTHPC/pCN is proposed.

g-C3N4 Modified by meso-Tetrahydroxyphenylchlorin for Photocatalytic Hydrogen Evolution Under Visible/Near-Infrared Light