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Selective oxidation of methane to methanol has been often considered as a “holy grail” reaction in catalysis. Herein, we systematically investigate the effect of solution pH and Pd-to-Au ratio of AuPd  x   colloid on the catalytic performance of methane oxidation. It is revealed that these two parameters can determine the amount of H 2 O 2  participated in the reaction, which is linearly related to the productivity of oxygenates. A high catalytic performance in methane activation requires a high utilization of H 2 O 2  to generate more ·OH. The optimal pH is 3.0 and the optimal Pd-to-Au ratio is between 0.1 to 0.7.

High H2O2 Utilization Promotes Selective Oxidation of Methane to Methanol at Low Temperature