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Two types of polynuclear Cd-Ln complexes [CdLnL(NO 3 )Cl 2 (DMF) 2 ] [Ln = La ( 1 ) and Nd ( 2 )] and [Ln 2 CdL 2 (NO 3 ) 2 (DMF) 2 ](OH) 2  [Ln = La ( 3 ) and Nd ( 4 )] were constructed using a new Schiff base ligand which has a long backbone with two phenyl groups. The Schiff base ligands show a “twist” configuration in  1 – 4 . The crystal structures show that the molecular dimensions of  3  and  4  are about 6 × 10 × 15 Å. The Cd-Nd complexes  2  and  4  exhibit the typical NIR luminescence of Nd 3+ . Interestingly,  4  shows the luminescent sensing of nitro explosives and exhibits a high sensitivity to 2-nitrophenol at the ppm level.

Anion Dependent Self-Assembly of Polynuclear Cd-Ln Schiff Base Nanoclusters: NIR Luminescent Sensing of Nitro Explosives