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The compounds of the Li3Sc2-xBx(PO4)3 system (where x=0•€2) were synthesized by a solid state reaction and studied by X-ray diffraction . For the investigation of electric properties the ceramic samples were sintered and the ceramic (x=0; 0.5; 1) and glass (x=2) samples were investigated in frequency range 106-1.2•E109 Hz at temperatures 300 600K . Two regions of the relaxation dispersion were found in conductivity spectra of the ceramics . They are related to the fast Li+ ion transport in the bulk and grain boundaries of the ceramics. The isomorphic substitution Sc• ̈B leads to the change of the temperature of phase transition to ƒÁphase (TƒÁ) . The increase of the stoichiometric factor x caused the increase of the values of bulk (GO and total (ƒÐtot) conductivities, and also decrease of their activation energies in the temperature range below TƒÁ.

phosphorus research bulletin

CHARACTERIZATION AND IMPEDANCE SPECTROSCOPY OF Li&lt;SUB&gt;3&lt;/SUB&gt;Sc&lt;SUB&gt;2-x&lt;/SUB&gt;B&lt;SUB&gt;x&lt;/SUB&gt;(PO&lt;SUB&gt;4&lt;/SUB&gt;)&lt;SUB&gt;3&lt;/SUB&gt; (WHERE x=0-2) SOLID ELECTROLYTE CERAMICS