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Methods of chemical preparation and crystallographic data are reported for two new condensed phosphates : a polyphosphate of nickel and cesium, NiCs4(PO3)6, and a cyclotriphosphate of nickel and potassium, NiK4(P3O9)2. NiCs4(PO3)6 is rhombohedral with the following unit-cell dimensions : a = b = 11.602(1)•ð, c = 9.078(1)•ð, space group P-31c, V = 1058.24(1)•ð3 and Z = 2. NiK4(P3O9)2 is triclinic with the following unit-cell dimensions : a = 6.143(8)•ð, b = 6.80(1)•ð, c = 12.80(3) •ð, a = 102.8(3)•‹,ƒÀ = 89.7(2)•‹,ƒÁ = 66.03(7)•‹, space group P-1, V = 473.56(3)•ð3 and Z = 1.

phosphorus research bulletin

CHEMICAL PREPARATION AND CRYSTAL DATA FOR TWO CONDENSED PHOSPHATES NiCs&lt;SUB&gt;4&lt;/SUB&gt;(PO&lt;SUB&gt;3&lt;/SUB&gt;)&lt;SUB&gt;6&lt;/SUB&gt; AND NiK&lt;SUB&gt;4&lt;/SUB&gt;(P&lt;SUB&gt;3&lt;/SUB&gt;O&lt;SUB&gt;9&lt;/SUB&gt;)&lt;SUB&gt;2&lt;/SUB&gt;