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Li1+xAlxGe2-x(PO4)3 (LAGP) solid electrolyte is one of the promising solid electrolytes for lithium ion batteries. The LAGP electrolyte was prepared by a sol-gel method. A gelation powder was calcined at 500 oC to obtain precursor powder for LAGP. The obtained powder was pelletized and calcined at 800, 850, and 900 oC. The pellets possessed NASICON structure, indicating that the LAGP was successfully prepared. The pellet calcined at 850 oC showed the highest lithium ion conductivity, 1.4 × 10-4 S cm-1, which is acceptable for all-solid-state lithium battery. Although some modification is still needed to improve the lithium ion conductivity of LAGP prepared by the sol-gel method, this finding provides us a new route for LAGP preparation.

phosphorus research bulletin

PREPARATION OF Li&lt;sub&gt;1.5&lt;/sub&gt;Al&lt;sub&gt;0.5&lt;/sub&gt;Ge&lt;sub&gt;1.5&lt;/sub&gt;(PO&lt;sub&gt;4&lt;/sub&gt;)&lt;sub&gt;3&lt;/sub&gt; SOLID ELECTROLYTE BY SOL-GEL METHOD