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In the tubular reactor, Hydrodesulfurization on the 7-ox-9-thiortricyclo[3.2.2.1]heptanes-5-ene-2,3-dicarboxylicacid(A) and Nordehydrocantharidin(B) have been accomplished for the first time in the presence of MoCo/γ-Al2O3 with the goal of obtaining pharmacologically promising Cantharidin-based molecules. The yields of Cantharidin(C) and Norcantharidin(D) were 71% and 80%. And the structure of compounds C and D was confirmed by H-NMR and C-NMR, NOESY and ESI-MS. We envisage that this process could be further developed at an industrial scale for the synthesis of Cantharidin-based molecules.

MoCo/γ-Al2O3-catalyzed hydrodesulfurization to synthesis of cantharidin-based molecules