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Multi-layered ceramic composites with alternation of grain sizes in layers were produced by adding thin interlayers of graphene-augmented alumina nanofibres (GAIN) between layers of monolithic α-Al2O3. The composite was mounted layer by layer directly in the graphite mould, using a vacuum filter system to precipitate alumina nanopowder and GAIN layers from the corresponding suspensions. The 30-mm diameter samples were consolidated by the spark plasma sintering technology at 1450 °C in nitrogen atmosphere at 50 MPa pressure. The effect of interlayers on the microstructure of alumina and on the thermal and electrical conductivity of the compact is studied.

Spark plasma sintering of layered γ-Al2O3/graphene reinforced nanocomposites

Spark plasma sintering of layered γ-Al₂O₃/graphene reinforced nanocomposites