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The formation of a single-phase nanocrystalline Hf 61 Fe 39  alloy with the fcc-Hf 2 Fe structure was achieved in a single step by melt-quenching, similarly to the previously reported nanocrystalline HfNi 5  phase in a melt-quenched Hf 11 Ni 89  alloy. Structural studies by X-ray diffraction and transmission electron microscopy have been performed for the nanocrystalline Hf 61 Fe 39  alloy in both the as-quenched state and after various heat treatments. It was found that the as-quenched state exhibits an average grain size of about 50 nm and a lattice parameter remarkably lower than the value known for the stoichiometric fcc-Hf 2 Fe phase.

Structure and thermal stability of a melt-quenched single-phase nanocrystalline Hf 61 Fe 39 alloy