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Phase equilibria were investigated for the Al-rich alloys Co 25-x Ni x Al 75  (0 ≤ x ≤ 25) and Co 22-y Ni y Al 78  (0 ≤ y ≤ 22). An addition of Ni to the Al-rich Co– Al alloys significantly decreases the binary peritectic, peritectoid and eutectoid temperatures. On the other hand, the temperature of the peritectic formation of NiAl 3  increases with increasing Co addition; the maximal solubility of Co in NiAl 3  amounts 10.5 at.% at 860 °C. Nickel substitutes Co in Co 2 Al 9  up to 4.7 at.%. The pseudoternary high-temperature phase (Co,Ni) 4 Al 13 (h) is stabilized by Ni addition up to 7 at.% Ni. The ternary phase Y 2  is formed by ternary peritectoid reaction from (Co,Ni) 4 Al 13  (h), Ni containing Co 2 Al 9  and the decagonal phase at 880 °C. It shows only a limited homogeneity range Co 17 Ni 8.2 Al 74.8  to Co 16.2 Ni 9 Al 74.8 .

Phase Equilibria in the Al-rich Portion of the Ternary System Co– Ni –Al at 75 and 78 at.% Al